Ultrasonically-Assisted Preparation and Functionalization of Graphene


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Since the extraordinary characteristics of graphite and graphene are known, several methods for its preparation have been developed. Beside to chemical production of graphenes from graphene oxide in multi-step processes, for which very strong oxidizing and reducing agents are needed. Additionally, the graphene prepared under these harsh chemical conditions often contain a large amount of defects even after reduction compared to graphenes obtained from other methods. However, ultrasound is a proven alternative to produce high quality graphene, also in large quantities. Researchers have developed different ways using ultrasound, but in general the graphene production is a simple one-step process. To give an example of a specific graphene production route: Graphite is added in a mixture of dilute organic acid, alcohol, and water, and then the mixture is exposed to ultrasonic irradiation. The acid works as a “molecular wedge” which separates sheets of graphene from the parent graphite. By this simple process, a large quantity of undamaged, high-quality graphene dispersed in water is created. (An et al. 2010)

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Journal: TechConnect Briefs
Volume: Technical Proceedings of the 2013 Clean Technology Conference and Trade Show
Published: May 12, 2013
Pages: 322 - 329
Industry sectors: Advanced Materials & Manufacturing | Energy & Sustainability
Topic: Catalysis
ISBN: 978-1-4822-0594-7